Production and Characterization of FeB and Fe2B Compounds by Mechanochemical Method

dc.contributor.authorCelik, Ulku Asli
dc.contributor.authorSunar, Talha
dc.contributor.authorOzyurek, Dursun
dc.contributor.authorGuru, Metin
dc.date.accessioned2024-09-29T16:06:50Z
dc.date.available2024-09-29T16:06:50Z
dc.date.issued2023
dc.departmentKarabük Üniversitesien_US
dc.description.abstractIn this study, iron and boron powders were alloyed at different rates (according to their molar weights) in a spex-type grinding device, and FeB and Fe2B compounds were obtained by mechanochemical method (the solid phase reaction). The containment and precise measurements of iron and boron mixed in different mole ratios were carried out with the Glove-Box in an argon atmosphere. Thermogravimetric and Differential Thermal Analysis for the determination of the sintering temperature of alloys; X-ray Diffraction and Scanning Electron Microscopy analyzes were performed to examine the phase compositions and microstructures. As a result of the studies, highly amorphous Fe2B and FeB compounds were produced. Due to the stoichiometric coefficients, the peaks of the FeB composition were more pronounced. For the sample targeted as FeB, it was observed that the peaks of the FeB composition were more pronounced due to the stoichiometric coefficients. From the EDS analysis, it was understood that the iron and boron elements on the surface of the samples exhibited a homogeneous distribution in the structure. According to the hardness results, it is understood that the sample targeted as FeB is harder than the samples targeted as Fe2B. This study will contribute to the production of advanced materials with regional hardness regimes by synthesizing different compositions.en_US
dc.identifier.doi10.2339/politeknik.1288108
dc.identifier.issn1302-0900
dc.identifier.issn2147-9429
dc.identifier.urihttps://doi.org/10.2339/politeknik.1288108
dc.identifier.urihttps://hdl.handle.net/20.500.14619/7068
dc.identifier.wosWOS:001192392600001en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.language.isoenen_US
dc.publisherGazi Univen_US
dc.relation.ispartofJournal of Polytechnic-Politeknik Dergisien_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectIron-boride compoundsen_US
dc.subjectmechanochemical methoden_US
dc.subjectsolid phase reactionen_US
dc.titleProduction and Characterization of FeB and Fe2B Compounds by Mechanochemical Methoden_US
dc.typeArticleen_US

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