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2-Ethyl-6,6-ethylenedisulfanediyl-7-methoxymethyl-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indol-3-one
(Int Union Crystallography, 2010) Tercan, Baris; Sahin, Ertan; Patir, Sueleyman; Hokelek, Tuncer
The title compound, C20H24N2O2S2, consists of a tetracyclic ring system containing an azocino skeleton with ethyl, dithiolane and methoxymethyl groups as substituents. The benzene and five-membered rings are nearly coplanar, with a dihedral angle of 2.78 (11)degrees. The dithiolane ring adopts an envelope conformation. In the crystal structure, intermolecular C-H center dot center dot center dot O hydrogen bonds link the molecules into chains nearly parallel to the c axis. Two C-H center dot center dot center dot pi interactions are also present.
6,6-[Ethylenebis(sulfanediyl)]-2-(2-methoxyethyl)-1,2,3,4,5,6-hexahydro-1,5-methano-1H-azocino[4,3-b]indol-3-one
(Int Union Crystallography, 2010) Tercan, Baris; Yuksel, Fatma; Patir, Sueleyman; Hokelek, Tuncer
The title compound, C19H22N2O2S2, consists of a tetracyclic ring system containing an azocine skeleton with methoxyethyl and dithiolane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)degrees. The dithiolane ring adopts an envelope conformation. Intermolecular N-H center dot center dot center dot O hydrogen-bonding and weak C-H center dot center dot center dot pi interactions are present in the crystal structure.