Novel phthalocyanines containing substituted salicyclic hydrazone-1,3-thiazole moieties: Microwave-assisted synthesis, spectroscopic characterization, X-ray structure and thermal characterization

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dc.authoridDegirmencioglu, Ismail/0000-0002-7964-0427
dc.contributor.authorDegirmencioglu, Ismail
dc.contributor.authorAtalay, Esra
dc.contributor.authorEr, Mustafa
dc.contributor.authorKoysal, Yavuz
dc.contributor.authorIsik, Samil
dc.contributor.authorSerbest, Kerim
dc.date.accessioned2024-09-29T15:55:16Z
dc.date.available2024-09-29T15:55:16Z
dc.date.issued2010
dc.departmentKarabük Üniversitesien_US
dc.description.abstractNovel, metal-free and metallo(Cu, Co, Ni, Zn, Pb and Mn)phthalocyanine compounds were synthesized by exposure to microwave irradiation and the products purified. The newly prepared compounds were characterized using elemental analyses, IR, H-1/C-13 NMR, H-1-H-1 COSY measurements, MS, UV-vis spectroscopy and DTA/TG analysis. The electronic spectra exhibited an intense pi -> pi* transition with characteristic Q and B bands of the phthalocyanine core, as expected. All decomposition products obtained from DTA/TG analysis were identified: it was found that the thermal stability of each phthalocyanine compound followed the order: MnPc < Metal-free < ZnPc < PbPc < CuPc < CoPc < NiPc. (C) 2009 Elsevier Ltd. All rights reserved.en_US
dc.description.sponsorshipResearch Fund of Karadeniz Technical University [2006.111.002.4]; TUBITAK [107T429]en_US
dc.description.sponsorshipThis study was supported by the Research Fund of Karadeniz Technical University, Project No: 2006.111.002.4 (Trabzon-Turkey) and supported by TUBITAK, Project No: 107T429.en_US
dc.identifier.doi10.1016/j.dyepig.2009.07.001
dc.identifier.endpage78en_US
dc.identifier.issn0143-7208
dc.identifier.issn1873-3743
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-69249203454en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage69en_US
dc.identifier.urihttps://doi.org/10.1016/j.dyepig.2009.07.001
dc.identifier.urihttps://hdl.handle.net/20.500.14619/4562
dc.identifier.volume84en_US
dc.identifier.wosWOS:000271375900009en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherElsevier Sci Ltden_US
dc.relation.ispartofDyes and Pigmentsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCharacterizationen_US
dc.subjectPhthalocyanineen_US
dc.subjectMicrowave irradiationen_US
dc.subjectHydrazoneen_US
dc.subjectSpectroscopyen_US
dc.subjectX-Rayen_US
dc.titleNovel phthalocyanines containing substituted salicyclic hydrazone-1,3-thiazole moieties: Microwave-assisted synthesis, spectroscopic characterization, X-ray structure and thermal characterizationen_US
dc.typeArticleen_US

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