catena-Poly[[[bis(4-ethylbenzoato-?2O,O')lead(II)]-?-nicotinamide-?2N1:O] monohydrate]

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dc.authoridHokelek, Tuncer/0000-0002-8602-4382
dc.authoridAKTAS, Vedat/0000-0003-3413-5424
dc.contributor.authorHokelek, Tuncer
dc.contributor.authorTercan, Baris
dc.contributor.authorSahin, Ertan
dc.contributor.authorAktas, Vedat
dc.contributor.authorNecefoglu, Hacali
dc.date.accessioned2024-09-29T16:03:22Z
dc.date.available2024-09-29T16:03:22Z
dc.date.issued2011
dc.departmentKarabük Üniversitesien_US
dc.description.abstractIn the crystal structure of the polymeric title compound, {[Pb(C9H9O2)(2)(C6H6N2O)]center dot H2O}(n), the six-coordinate Pb-II ion is chelated by two 4-ethylbenzoate (PEB) anions and is bridged by two nicotinamide (NA) ligands, forming a polymeric chain running along the b axis. The carboxylate groups of the PEB ions are twisted away from the attached benzene rings by 4.0 (6) and 13.3 (5)degrees. The two benzene rings of the PEB ions bonded to the same metal ion are oriented at a dihedral angle of 87.4 (3) . In the polymeric chain, the N-A ligand is linked to one of the carboxylate groups via N-H center dot center dot center dot O hydrogen bonding. In the crystal, adjacent polymeric chains interact via N-H center dot center dot center dot O and weak C-H center dot center dot center dot O hydrogen bonds; and the lattice water molecule links with the polymeric chains via N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonding. pi-pi stacking between the benzene and the pyridine rings [centroid-centroid distance = 3.805 (5) angstrom] and weak C-H center dot center dot center dot center dot pi interactions are also observed in the crystal structure.en_US
dc.description.sponsorshipUniversity Research Fund [2003/219]en_US
dc.description.sponsorshipThe authors are indebted to the Department of Chemistry, Ataturk University, Erzurum, Turkey, for the use of X-ray diffractometer purchased under grant No. 2003/219 of the University Research Fund.en_US
dc.identifier.doi10.1107/S1600536811026535
dc.identifier.endpageU550en_US
dc.identifier.issn2056-9890
dc.identifier.pmid22090843en_US
dc.identifier.scopus2-s2.0-80051520542en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpageM1057en_US
dc.identifier.urihttps://doi.org/10.1107/S1600536811026535
dc.identifier.urihttps://hdl.handle.net/20.500.14619/6036
dc.identifier.volume67en_US
dc.identifier.wosWOS:000294613900037en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherInt Union Crystallographyen_US
dc.relation.ispartofActa Crystallographica Section E-Structure Reports Onlineen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectMonohydrateen_US
dc.titlecatena-Poly[[[bis(4-ethylbenzoato-?2O,O')lead(II)]-?-nicotinamide-?2N1:O] monohydrate]en_US
dc.typeArticleen_US

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