Obtainment of Copper(II) Fluoroborate by High-Energy Impacted Ball-Milling
dc.contributor.author | Aydin, D. Y. | |
dc.contributor.author | Guru, M. | |
dc.contributor.author | Ipek, D. | |
dc.contributor.author | Ozyurek, D. | |
dc.date.accessioned | 2024-09-29T16:05:15Z | |
dc.date.available | 2024-09-29T16:05:15Z | |
dc.date.issued | 2019 | |
dc.department | Karabük Üniversitesi | en_US |
dc.description | 8th International Advances in Applied Physics and Materials Science Congress and Exhibition (APMAS) -- APR 24-30, 2018 -- Fethiye, TURKEY | en_US |
dc.description.abstract | In this study, copper(II) fluoroborate, one of the special boron products, was synthesized by high energy impacted ball milling method and characterization studies were carried out by means of FTIR and BF4- ion selective electrode. Copper fluoride and elemental boron were used as reactants in the study. Mechanochemical method by means of ball milling was carried out, in a three-dimensional spex-type ball mill in an argon atmosphere. Specimens were prepared at different mole ratios and mechanically milled in a ball mill for a fixed time to determine the optimum mole ratio and the reaction period was optimized in the next step. As a result of the experiments, the most efficient reaction was obtained when reactant mole ratio (n(B)/n(CuF2)) of 0.85:1 and reaction period of 1500 minutes. Copper(II) fluoroborate was produced with a yield of 84.5% under the optimum conditions. | en_US |
dc.description.sponsorship | Eti Mine Works General Managements [2014.C.11.0010.15]; Eti Mine Works of Turkey | en_US |
dc.description.sponsorship | This work was supported by Eti Mine Works General Managements under Project Number 2014.C.11.0010.15. The authors are grateful to Eti Mine Works of Turkey for financial support and Gazi University for laboratory facilities usage. | en_US |
dc.identifier.doi | 10.12693/APhysPolA.135.888 | |
dc.identifier.endpage | 891 | en_US |
dc.identifier.issn | 0587-4246 | |
dc.identifier.issn | 1898-794X | |
dc.identifier.issue | 5 | en_US |
dc.identifier.scopus | 2-s2.0-85071155817 | en_US |
dc.identifier.scopusquality | Q4 | en_US |
dc.identifier.startpage | 888 | en_US |
dc.identifier.uri | https://doi.org/10.12693/APhysPolA.135.888 | |
dc.identifier.uri | https://hdl.handle.net/20.500.14619/6599 | |
dc.identifier.volume | 135 | en_US |
dc.identifier.wos | WOS:000481717400009 | en_US |
dc.identifier.wosquality | Q4 | en_US |
dc.indekslendigikaynak | Web of Science | en_US |
dc.indekslendigikaynak | Scopus | en_US |
dc.language.iso | en | en_US |
dc.publisher | Polish Acad Sciences Inst Physics | en_US |
dc.relation.ispartof | Acta Physica Polonica A | en_US |
dc.relation.publicationcategory | Konferans Öğesi - Uluslararası - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/openAccess | en_US |
dc.subject | Tetrafluoroborate | en_US |
dc.subject | Catalyst | en_US |
dc.title | Obtainment of Copper(II) Fluoroborate by High-Energy Impacted Ball-Milling | en_US |
dc.type | Conference Object | en_US |