Ethyl 2-[2-(4-hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]-3,4-dimethyl-2,3-dihydro-1,3-thiazole-5-carboxylate

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dc.contributor.authorYildirim, Sema Ozturk
dc.contributor.authorButcher, Ray J.
dc.contributor.authorKoysal, Yavuz
dc.contributor.authorKantar, Esen Nur
dc.contributor.authorBelder, Ayse
dc.date.accessioned2024-09-29T16:03:22Z
dc.date.available2024-09-29T16:03:22Z
dc.date.issued2012
dc.departmentKarabük Üniversitesien_US
dc.description.abstractThe title compound, C16H19N3O4S, is almost planar, with a dihedral angle of 2.88 (9)degrees between the mean planes of the benzene and thiazole rings. The molecule adopts an E conformation about the two C = N bonds, with a C-N-N- C torsion angle of -177.01 (11)degrees. An intramolecular CH center dot center dot center dot O hydrogen bond exists between a thiazole methyl group and the formic acid ethyl ester carbonyl O atom. In the crystal, molecules are linked by O-H center dot center dot center dot O hydrogen bonds, forming chains propagating along [210]. The chains are linked via CH center dot center dot center dot O hydrogen bonds with R-2(2) (12) ring motifs, forming sheets lying parallel to (122). The sheets are further linked through out-of-plane C-H center dot center dot center dot N hydrogen bonds with R-2(2) (12) ring motifs and C-H center dot center dot center dot pi nteractions, forming an interesting three-dimensional supramolecular architecture.en_US
dc.description.sponsorshipNSF-MRI program [CHE-0619278]en_US
dc.description.sponsorshipRJB acknowledges the NSF-MRI program (grant No. CHE-0619278) for funds to purchase the diffractometer.en_US
dc.identifier.doi10.1107/S1600536812043772
dc.identifier.endpage+en_US
dc.identifier.issn2056-9890
dc.identifier.pmid23284520en_US
dc.identifier.scopus2-s2.0-84870916284en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpageO3213en_US
dc.identifier.urihttps://doi.org/10.1107/S1600536812043772
dc.identifier.urihttps://hdl.handle.net/20.500.14619/6037
dc.identifier.volume68en_US
dc.identifier.wosWOS:000421552000210en_US
dc.identifier.wosqualityN/Aen_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherInt Union Crystallographyen_US
dc.relation.ispartofActa Crystallographica Section E-Structure Reports Onlineen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.titleEthyl 2-[2-(4-hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]-3,4-dimethyl-2,3-dihydro-1,3-thiazole-5-carboxylateen_US
dc.typeArticleen_US

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