Investigation of thermal and magnetic properties of [MSalen/Saloph] (M = Cr3+, Fe3+ or Co3+) capped dinuclear complexes of two novel tetraoxocalix[2]arene[2]triazine ligands
dc.authorid | UYSAL, Saban/0000-0003-1061-6143 | |
dc.contributor.author | Aouled, Idriss Mahamoud | |
dc.contributor.author | Uysal, Saban | |
dc.date.accessioned | 2024-09-29T16:00:26Z | |
dc.date.available | 2024-09-29T16:00:26Z | |
dc.date.issued | 2023 | |
dc.department | Karabük Üniversitesi | en_US |
dc.description.abstract | In this study, tetraoxocalix[2]arene[2]triazine compound as starting compound codded as C1 was synthesized by reacting of 2,4,6-trichloro-1,3,5-triazine with methyl-3,5-dihydroxybenzoate in two stages. sTriazine bridged calixarene ligands as target ligands, which we coded as C2 and C3, were obtained from the reaction of C1 coded compound with 4-aminobenzoic acid or 4-hydroxybenzoic acid at 1:2 mole ratio, respectively. [MSalen/Saloph] capped benzoic acid substitute tetraoksocalix[2] aren[2]triazine complexes were obtained from the reaction of C2 or C3 codded ligand with [(MSalen/Saloph) 2 O] (M = Cr 3 + , Fe 3 + and Co 3 + ) starting complexes in 1,4-dioxane media. The ligands obtained were characterized by using 1 HNMR , FT-IR spectroscopy and elemental analysis techniques. The complexes obtained were characterized by using FT-IR, UV-vis spectroscopies, elemental analysis, magnetic susceptibility, and TGA-DTA techniques. Metal contents of the complexes were determined by using ICP-OES spectroscopy. (c) 2023 Elsevier B.V. All rights reserved. | en_US |
dc.description.sponsorship | Karabuk University Scientific Research Projects Coordinatorship [FYL-2020-2189] | en_US |
dc.description.sponsorship | We acknowledge that this study was financially supported by the Karabuk University Scientific Research Projects Coordinatorship (Project No: FYL-2020-2189) . | en_US |
dc.identifier.doi | 10.1016/j.molstruc.2023.135084 | |
dc.identifier.issn | 0022-2860 | |
dc.identifier.issn | 1872-8014 | |
dc.identifier.scopus | 2-s2.0-85147541910 | en_US |
dc.identifier.scopusquality | Q2 | en_US |
dc.identifier.uri | https://doi.org/10.1016/j.molstruc.2023.135084 | |
dc.identifier.uri | https://hdl.handle.net/20.500.14619/5140 | |
dc.identifier.volume | 1280 | en_US |
dc.identifier.wos | WOS:000932623900001 | en_US |
dc.identifier.wosquality | Q2 | en_US |
dc.indekslendigikaynak | Web of Science | en_US |
dc.indekslendigikaynak | Scopus | en_US |
dc.language.iso | en | en_US |
dc.publisher | Elsevier | en_US |
dc.relation.ispartof | Journal of Molecular Structure | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | s-Triazine bridged calixarene complexes | en_US |
dc.subject | Calix[2]arene[2]triazines | en_US |
dc.subject | Schiff Base | en_US |
dc.subject | Salen | en_US |
dc.subject | Saloph | en_US |
dc.title | Investigation of thermal and magnetic properties of [MSalen/Saloph] (M = Cr3+, Fe3+ or Co3+) capped dinuclear complexes of two novel tetraoxocalix[2]arene[2]triazine ligands | en_US |
dc.type | Article | en_US |