The synthesis and characterization of s-triazine bridged calixarene based a Schiff base: Investigation of its [MSalen/Salophen] (M = Cr3+, Fe3+ or Co3+) capped complexes

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dc.authoridUYSAL, Saban/0000-0003-1061-6143
dc.contributor.authorAouled, Idriss Mahamoud
dc.contributor.authorUysal, Saban
dc.date.accessioned2024-09-29T16:00:26Z
dc.date.available2024-09-29T16:00:26Z
dc.date.issued2022
dc.departmentKarabük Üniversitesien_US
dc.description.abstractIn this study, 2,4-bis((4,6-dichloro-1,3,5-triazin-2-yl)oxy)benzaldehyde, was obtained by reacting cyanuric chloride with 2,4-dihydroxybenzaldehyde at 0 degrees C. Then, s-triazine bridged calixarene codded as TABCA1 was obtained by reacting the compounds with 2,4-dihydroxybenzaldehide. This s-triazine bridged calixarene ligand, which we coded as TABCA2, was obtained from the reaction of TABCA1 coded compound with 4-aminobenzoic acid at a 1:2 mole ratio, twice. [MSalen/Saloph] capped s-triazine bridged calixaren complexes were obtained from the reaction of TABCA2 codded ligand and the [(MSalen/Saloph)(2)O] (M=Cr3+, Fe3+ and Co3+) starting complexes in 1,4-dioxane media. The ligand obtained were characterized by using H-1 NMR, FT-IR spectroscopy and elemental analysis techniques. The complexes obtained were characterized by using FT-IR, UV-Vis spectroscopies, elemental analysis, magnetic susceptibility, and TGA-DTA techniques. Metal contents of the complexes were determined by using ICP-AES spectroscopy. (C) 2021 Elsevier B.V. All rights reserved.en_US
dc.description.sponsorshipKarabuk University Scientific Research Projects Coordinatorship [FYL-2020-2189]en_US
dc.description.sponsorshipWe acknowledge that this study was financially supported by the Karabuk University Scientific Research Projects Coordinatorship (Project No: FYL-2020-2189).en_US
dc.identifier.doi10.1016/j.molstruc.2021.131872
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.scopus2-s2.0-85119104806en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2021.131872
dc.identifier.urihttps://hdl.handle.net/20.500.14619/5138
dc.identifier.volume1250en_US
dc.identifier.wosWOS:000744651100007en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Molecular Structureen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectS-triazine bridged calixareneen_US
dc.subjectS-triazine bridged calixarene complexesen_US
dc.subjectCalix[2]aren[2]triazinesen_US
dc.subjectSchiffbaseen_US
dc.subjectSalenen_US
dc.subjectSalophen_US
dc.titleThe synthesis and characterization of s-triazine bridged calixarene based a Schiff base: Investigation of its [MSalen/Salophen] (M = Cr3+, Fe3+ or Co3+) capped complexesen_US
dc.typeArticleen_US

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